5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole

Basavegowda Nagaraj; Rajenahally S. Narasegowda; Hemmige S. Yathirajan; Santhosh L. Gaonkar; Michael Bolte

doi:10.1107/S1600536805005490

5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole

Basavegowda Nagaraj
, Rajenahally S. Narasegowda
, Hemmige S. Yathirajan
, Santhosh L. Gaonkar
, Michael Bolte^*

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

3 Citations (Scopus)

Abstract

The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.

Original language	English
Pages (from-to)	o767-o768
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	61
Issue number	3
DOIs	https://doi.org/10.1107/S1600536805005490
Publication status	Published - 03-2005

All Science Journal Classification (ASJC) codes

General Chemistry
General Materials Science
Condensed Matter Physics

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title = "5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole",

abstract = "The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.",

author = "Basavegowda Nagaraj and Narasegowda, \{Rajenahally S.\} and Yathirajan, \{Hemmige S.\} and Gaonkar, \{Santhosh L.\} and Michael Bolte",

year = "2005",

month = mar,

doi = "10.1107/S1600536805005490",

language = "English",

volume = "61",

pages = "o767--o768",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "3",

}

TY - JOUR

T1 - 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole

AU - Nagaraj, Basavegowda

AU - Narasegowda, Rajenahally S.

AU - Yathirajan, Hemmige S.

AU - Gaonkar, Santhosh L.

AU - Bolte, Michael

PY - 2005/3

Y1 - 2005/3

N2 - The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.

AB - The synthesis of 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole, was studied. The 5-(4′-Methylbiphenyl-2-yl)-1H-tetrezole, trityl chloride and triethylamine in dichloromethane were stirred for 2 hours at room temperature. To obtain the compound the recovered product was treated with 1-bromo2,5-pyrrolidinedione and benzoyal peroxide in carbon tetrachloride. It is observed that the compound 5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole is recrystallized from ethyl methyl ketone.

UR - https://www.scopus.com/pages/publications/18544363274

UR - https://www.scopus.com/pages/publications/18544363274#tab=citedBy

U2 - 10.1107/S1600536805005490

DO - 10.1107/S1600536805005490

M3 - Article

AN - SCOPUS:18544363274

SN - 1600-5368

VL - 61

SP - o767-o768

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 3

ER -

5-[4′-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole

Abstract

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