Redetermination of methyl 3,4-O-isopropyl-idene-Β-D-fucopyran-oside monohydrate

Hoong Kun Fun; Samuel Robinson Jebas; Sankappa Rai; Prakash Shetty; Arun M. Isloor

doi:10.1107/S1600536809012689

Redetermination of methyl 3,4-O-isopropyl-idene-Β-D-fucopyran-oside monohydrate

Hoong Kun Fun^*
, Samuel Robinson Jebas
, Sankappa Rai
, Prakash Shetty
, Arun M. Isloor

^*Corresponding author for this work

Research output: Contribution to journal › Article › peer-review

Abstract

In the title compound, C₁₀H₁₈O₅· H₂O, the fucopyran-oside ring adopts a chair conformation. The crystal packing is stabilized by inter-molecular O - H⋯O and C - H⋯O hydrogen bonds together with intra-molecular O⋯O [2.2936 (8) Å] and inter-molecular O⋯O [2.7140 (8)-2.829 (3) Å] short contacts. The mol-ecules are linked together to form an infinite chain along the a axis. This structure has been solved previously but with no R-values [Spiers (1931). Z. Kristallogr. Kristallgeom. Kristallphys. Kristallchem. 78, 101].

Original language	English
Pages (from-to)	o1002-o1003
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	65
Issue number	5
DOIs	https://doi.org/10.1107/S1600536809012689
Publication status	Published - 15-06-2009

All Science Journal Classification (ASJC) codes

General Chemistry
General Materials Science
Condensed Matter Physics

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@article{28e0cf5d55834cd58982474aff856ad6,

title = "Redetermination of methyl 3,4-O-isopropyl-idene-Β-D-fucopyran-oside monohydrate",

abstract = "In the title compound, C10H18O5· H2O, the fucopyran-oside ring adopts a chair conformation. The crystal packing is stabilized by inter-molecular O - H⋯O and C - H⋯O hydrogen bonds together with intra-molecular O⋯O [2.2936 (8) {\AA}] and inter-molecular O⋯O [2.7140 (8)-2.829 (3) {\AA}] short contacts. The mol-ecules are linked together to form an infinite chain along the a axis. This structure has been solved previously but with no R-values [Spiers (1931). Z. Kristallogr. Kristallgeom. Kristallphys. Kristallchem. 78, 101].",

author = "Fun, \{Hoong Kun\} and Jebas, \{Samuel Robinson\} and Sankappa Rai and Prakash Shetty and Isloor, \{Arun M.\}",

year = "2009",

month = jun,

day = "15",

doi = "10.1107/S1600536809012689",

language = "English",

volume = "65",

pages = "o1002--o1003",

journal = "Acta Crystallographica Section E: Structure Reports Online",

issn = "1600-5368",

publisher = "International Union of Crystallography",

number = "5",

}

TY - JOUR

T1 - Redetermination of methyl 3,4-O-isopropyl-idene-Β-D-fucopyran-oside monohydrate

AU - Fun, Hoong Kun

AU - Jebas, Samuel Robinson

AU - Rai, Sankappa

AU - Shetty, Prakash

AU - Isloor, Arun M.

PY - 2009/6/15

Y1 - 2009/6/15

N2 - In the title compound, C10H18O5· H2O, the fucopyran-oside ring adopts a chair conformation. The crystal packing is stabilized by inter-molecular O - H⋯O and C - H⋯O hydrogen bonds together with intra-molecular O⋯O [2.2936 (8) Å] and inter-molecular O⋯O [2.7140 (8)-2.829 (3) Å] short contacts. The mol-ecules are linked together to form an infinite chain along the a axis. This structure has been solved previously but with no R-values [Spiers (1931). Z. Kristallogr. Kristallgeom. Kristallphys. Kristallchem. 78, 101].

AB - In the title compound, C10H18O5· H2O, the fucopyran-oside ring adopts a chair conformation. The crystal packing is stabilized by inter-molecular O - H⋯O and C - H⋯O hydrogen bonds together with intra-molecular O⋯O [2.2936 (8) Å] and inter-molecular O⋯O [2.7140 (8)-2.829 (3) Å] short contacts. The mol-ecules are linked together to form an infinite chain along the a axis. This structure has been solved previously but with no R-values [Spiers (1931). Z. Kristallogr. Kristallgeom. Kristallphys. Kristallchem. 78, 101].

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DO - 10.1107/S1600536809012689

M3 - Article

AN - SCOPUS:66749128537

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SP - o1002-o1003

JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

IS - 5

ER -

Redetermination of methyl 3,4-O-isopropyl-idene-Β-D-fucopyran-oside monohydrate

Abstract

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