Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one

G. B. Thippeswamy; D. Vijaykumar; B. S. Jayashree; M. A. Sridhar; J. Shashidhara Prasad

doi:10.1063/1.3605793

Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one

G. B. Thippeswamy, D. Vijaykumar, B. S. Jayashree, M. A. Sridhar, J. Shashidhara Prasad

Department of Pharmaceutical Chemistry, Manipal College of Pharmaceutical Sciences, Manipal

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

Abstract

The title compound, C1₄H1₀Cl₂O3, was synthesized and recrystallized from an organic solution and crystallizes in monoclinic system with space group P 21/c. The crystal structure analysis and the molecular arrangement of these crystals are determined using X-ray diffraction method. The molecule is almost planar as evidenced by the very low values of torsion angles. The hydroxy group substituted at C16 position is in anti-periplanar conformation with respect to the phenyl ring.

Original language	English
Title of host publication	Solid State Physics - Proceedings of the 55th DAE Solid State Physics Symposium 2010
Pages	176-177
Number of pages	2
Volume	1349
Edition	PART A
DOIs	https://doi.org/10.1063/1.3605793
Publication status	Published - 12-09-2011
Event	55th DAE Solid State Physics Symposium 2010 - Manipal, India Duration: 26-12-2010 → 30-12-2010

Conference

Conference	55th DAE Solid State Physics Symposium 2010
Country/Territory	India
City	Manipal
Period	26-12-10 → 30-12-10

All Science Journal Classification (ASJC) codes

Physics and Astronomy(all)

Access to Document

10.1063/1.3605793

Cite this

@inproceedings{11c50403cf7f45d0b943c8a2e71aa20b,

title = "Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one",

abstract = "The title compound, C14H10Cl2O3, was synthesized and recrystallized from an organic solution and crystallizes in monoclinic system with space group P 21/c. The crystal structure analysis and the molecular arrangement of these crystals are determined using X-ray diffraction method. The molecule is almost planar as evidenced by the very low values of torsion angles. The hydroxy group substituted at C16 position is in anti-periplanar conformation with respect to the phenyl ring.",

author = "Thippeswamy, {G. B.} and D. Vijaykumar and Jayashree, {B. S.} and Sridhar, {M. A.} and Prasad, {J. Shashidhara}",

year = "2011",

month = sep,

day = "12",

doi = "10.1063/1.3605793",

language = "English",

isbn = "9780735409057",

volume = "1349",

pages = "176--177",

booktitle = "Solid State Physics - Proceedings of the 55th DAE Solid State Physics Symposium 2010",

edition = "PART A",

note = "55th DAE Solid State Physics Symposium 2010 ; Conference date: 26-12-2010 Through 30-12-2010",

}

Thippeswamy, GB, Vijaykumar, D, Jayashree, BS, Sridhar, MA & Prasad, JS 2011, Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one. in Solid State Physics - Proceedings of the 55th DAE Solid State Physics Symposium 2010. PART A edn, vol. 1349, pp. 176-177, 55th DAE Solid State Physics Symposium 2010, Manipal, India, 26-12-10. https://doi.org/10.1063/1.3605793

Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one. / Thippeswamy, G. B.; Vijaykumar, D.; Jayashree, B. S. et al.
Solid State Physics - Proceedings of the 55th DAE Solid State Physics Symposium 2010. Vol. 1349 PART A. ed. 2011. p. 176-177.

Research output: Chapter in Book/Report/Conference proceeding › Conference contribution

TY - GEN

T1 - Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one

AU - Thippeswamy, G. B.

AU - Vijaykumar, D.

AU - Jayashree, B. S.

AU - Sridhar, M. A.

AU - Prasad, J. Shashidhara

PY - 2011/9/12

Y1 - 2011/9/12

N2 - The title compound, C14H10Cl2O3, was synthesized and recrystallized from an organic solution and crystallizes in monoclinic system with space group P 21/c. The crystal structure analysis and the molecular arrangement of these crystals are determined using X-ray diffraction method. The molecule is almost planar as evidenced by the very low values of torsion angles. The hydroxy group substituted at C16 position is in anti-periplanar conformation with respect to the phenyl ring.

AB - The title compound, C14H10Cl2O3, was synthesized and recrystallized from an organic solution and crystallizes in monoclinic system with space group P 21/c. The crystal structure analysis and the molecular arrangement of these crystals are determined using X-ray diffraction method. The molecule is almost planar as evidenced by the very low values of torsion angles. The hydroxy group substituted at C16 position is in anti-periplanar conformation with respect to the phenyl ring.

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U2 - 10.1063/1.3605793

DO - 10.1063/1.3605793

M3 - Conference contribution

AN - SCOPUS:80052435008

SN - 9780735409057

VL - 1349

SP - 176

EP - 177

BT - Solid State Physics - Proceedings of the 55th DAE Solid State Physics Symposium 2010

T2 - 55th DAE Solid State Physics Symposium 2010

Y2 - 26 December 2010 through 30 December 2010

ER -

Synthesis and crystal structure of 1-(3,5-dichloro-2-hydroxyphenyl)-3-(5- methylfuran-2-yl)prop-2-en-1-one

Abstract

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