Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

T. N. Mahadeva Prasad; S. L. Gaonkar; Kamini Kapoor; Vivek K. Gupta; H. Shimizu; M. A. Sridhar; J. Shashidhara Prasad

doi:10.2116/xraystruct.28.25

Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

T. N. Mahadeva Prasad
, S. L. Gaonkar
, Kamini Kapoor
, Vivek K. Gupta
, H. Shimizu
, M. A. Sridhar^*
, J. Shashidhara Prasad

^*Corresponding author for this work

Research output: Contribution to journal › Comment/debate › peer-review

1 Citation (Scopus)

Abstract

The title compound, C ₁₅H ₁₇N ₃O ₂, was synthesized, and the structure was characterised spectroscopically by ¹H NMR and ¹³C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å ³. 2012

Original language	English
Pages (from-to)	25-26
Number of pages	2
Journal	X-ray Structure Analysis Online
Volume	28
Issue number	4
DOIs	https://doi.org/10.2116/xraystruct.28.25
Publication status	Published - 2012

All Science Journal Classification (ASJC) codes

Analytical Chemistry
Materials Chemistry

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@article{4ac1342f29aa473ea3a1da4aa51a9eb6,

title = "Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime",

abstract = "The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8){\AA}, b = 8.6358(7){\AA}, c = 11.7675{\AA}, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11){\AA} 3. 2012",

author = "\{Mahadeva Prasad\}, \{T. N.\} and Gaonkar, \{S. L.\} and Kamini Kapoor and Gupta, \{Vivek K.\} and H. Shimizu and Sridhar, \{M. A.\} and \{Shashidhara Prasad\}, J.",

year = "2012",

doi = "10.2116/xraystruct.28.25",

language = "English",

volume = "28",

pages = "25--26",

journal = "X-ray Structure Analysis Online",

issn = "1883-3578",

publisher = "Japan Society for Analytical Chemistry",

number = "4",

}

TY - JOUR

T1 - Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

AU - Mahadeva Prasad, T. N.

AU - Gaonkar, S. L.

AU - Kapoor, Kamini

AU - Gupta, Vivek K.

AU - Shimizu, H.

AU - Sridhar, M. A.

AU - Shashidhara Prasad, J.

PY - 2012

Y1 - 2012

N2 - The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å 3. 2012

AB - The title compound, C 15H 17N 3O 2, was synthesized, and the structure was characterised spectroscopically by 1H NMR and 13C NMR methods, and finally confirmed by an X-ray diffraction study. The compound crystallizes in the triclinic crystal class in the space group Pī with the following cell parameters: a = 7.3332(8)Å, b = 8.6358(7)Å, c = 11.7675Å, α = 75.306(8)°, β = 73.835(9)°, γ = 89.698(8)°, Z = 2 and V = 690.63(11)Å 3. 2012

UR - https://www.scopus.com/pages/publications/84864152236

UR - https://www.scopus.com/pages/publications/84864152236#tab=citedBy

U2 - 10.2116/xraystruct.28.25

DO - 10.2116/xraystruct.28.25

M3 - Comment/debate

AN - SCOPUS:84864152236

SN - 1883-3578

VL - 28

SP - 25

EP - 26

JO - X-ray Structure Analysis Online

JF - X-ray Structure Analysis Online

IS - 4

ER -

Synthesis and crystal structure of 4-[2-(Methyl-pyridin2-ylamino)ethoxy]-benzaldoxime

Abstract

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